Certificate of Analysis / Certificat d analyse

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1 Date: (YYYY-MM-DD / AAAA-MM-JJ) Certificate of Analysis / Certificat d analyse Product code / Code du produit: Batch No. / No. de lot: Trade name / Nom commercial: Botanical name / Nom botanique: INCI name / Nom INCI: Use of product / Utilisation: Country of origin / Pays d origine: Certification: VHE007B MP Essential Oil of Angelica - Root / Huile essentielle d angélique - racine Angelica archangelica ANGELICA ARCHANGELICA ROOT OIL Cosmetic / Cosmétique Hungary / Hongrie Ecocert Canada Organic / Biologique Ecocert Canada 1. Method of production / Méthode d obtention Essential Oil obtained by steam distillation of the root of Angelica archangelica. / Huile essentielle obtenue par distillation à la vapeur d'eau de la racine d Angelica archangelica. 2. Certificate of Purity and Origin / Certificat de pureté et d origine - 100% pure and natural without any additive / 100% pur et naturel sans aucun additif - Certified Hungary origin / Origine Hongrie certifiée. 3. Organoleptic and Physical Properties / Caractéristiques organoleptiques et physiques Requirements / Spécifications Results /Résultats Physical appearance / Aspect physique: Liquid / Liquide Compliant /Conforme Colour / Couleur: Pale yellow to brown / Jaune pâle à brun Compliant /Conforme Odor / Odeur: Aromatic, warm and herbaceous / Aromatique, chaude et herbacée Compliant /Conforme Specific Gravity at 68ºF (20ºC) / Densité à 20ºC: 0,850 to/à 0,920 0,857 Refractive Index at 68ºF (20ºC) / Indice de réfraction à 20ºC: 1,470 to/à 1,488 1,475 Optical Rotation at 68ºF (20ºC) / Pouvoir rotatoire à 20ºC: +5 to/à , /5

2 4. Analysis Properties / Caractéristiques d analyse 4.1 Chromatographic Profile / Profil chromatographique - 2/5

3 4.2 Operating Conditions / Conditions opératoires Gas chromatograph : CPG/FID 6890 Chromatographe gazeux : CPG/FID 6890 Column Apolar : DB5 MS 20m 0,18 mm 0,18μm Colonne Apolaire : DB5 MS : 20 m 0,18 mm 0,18 µm Temperature Programming 50 C for 3.2min 10 C/min C at 300 C Gas vector : H2 : 0.9ml/min Sample : 4% of solution in acetone or hexane Injection volume : 1μl Programmation de température : 50 C pendant 3.2min 10 C/min C jusqu à 300 C Gaz vecteur : H2 : 0,9ml/min Échantillon : 4% en solution dans l acétone ou l hexane Volume d injection : 1μl Injector : 280 C with split 1/120 Injecteur : 280 C avec diviseur 1/120 The % is calculated from the peaks area given by the GC/FID without the use of correction factor Les % sont calculés à partir des surfaces de pics donnés par le GC/FID sans l utilisation de facteur de correction Gas chromatograph : CPG/MS 7890/5975C Chromatographe gazeux : CPG/MS 7890/5975C Column : Apolar : DB5 MS 20m 0,18 mm 0,18μm Colonne : Apolaire : DB5 MS : 20 m 0,18 mm 0,18 µm Temperature Programming: 50 C for 3.2min 8 C/min C at 300 C Gas Vector : He : 1ml/min Sample : 4% of solution in acetone or hexane Injection volume : 1μl Programmation de température : 50 C pdt 3,2min 8 C/min C jusqu à 300 C Gaz vecteur : He : 1ml/min Échantillon : 4% en solution dans l acétone ou l hexane Volume d injection : 1μl Injector : 280 C with split 1/150 Injecteur : 280 C avec diviseur 1/150 Mass Range : 33 to 550 Gamme de masse : 33 à 550 The components of the oil are identified by a combined search of retention times (lab library) and mass spectra (Library NIST records). Les composés de l huile sont identifiés par une recherche combinée des temps de rétention (bibliothèque du laboratoire) et des spectres de masse (librairie NIST spectres) - 3/5

4 4.3 Chromatographic analysis (GC/FID) / Analyse chromatographique (CG/FID) Main Constituents Results Table /1 Tableau 1 des résultats des principaux constituants Retention Times / Temps de rétention Constituents / Constituants Fid % 4.64 Tricyclene Alpha-Thujene Alpha-Pinene Camphene Thuja-2,4(10)-diene Sabinene Beta-Pinene Myrcene Carene-2-Delta Mentha-1(7),8-diene Alpha-Phellandrene Carene-3-Delta Alpha-Terpinene Ortho-Cymene Para-Cymene Limonene Beta-Phellandrene (Z)-Béta-Ocimene (E)-Béta-Ocimene Gamma-Terpinene Terpinolene-Isomer Terpinolene Para-Cymenene Linalool Cis-Para-Menth-2-ene-1-ol Trans-Para-Menth-2-ene-1-ol Pentyl-Cyclo-Hexadiene-1, Terpinene-4-ol Para-Cymene-8-ol Myrtenal Cis-Piperitol Trans-Piperitol Bornyl Acetate Trans-Sabinyl Acetate Cyclosativene Note: The allergens are identified in bold / Les allergènes sont identifies en caractères gras /5

5 4.3.2 Main Constituents Results Table 2 / Tableau 2 des résultats des principaux constituants Retention Times / Temps de rétention Constituents / Constituants Fid % Alpha-Copaene Beta-Elemene Beta-Caryophyllene Gamma-Elemene (Z)-Béta-Farnesene Alpha-Humulene Germacrene-D Alpha-Zingiberene Alpha-Muurolene Beta-Bisabolene Delta-Cadinene Alpha-Copaene-ol Germacrene-B Caryophyllene Oxide Tridecanolide Exaltolide Osthol Total Note: The allergens are identified in bold / Les allergènes sont identifies en caractères gras. Analysis Date / Date de l analyse: Tomas Seijas, Chemist/Chimiste, OCQ # /5

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