REACH Chemical Analysis. TiWi-C-W

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1 TiWi-C-W Last updated February 9, R1.1 Copyright 2015 LS Research Page 1 of 13

2 1.1 Table of Contents REACH Chemical Analysis... 1 TiWi-C-W 1 1 General Information Summary Date of Test Test Laboratory Description of Sample Definitions Revision History Measurement Flow Chart Chemical Analysis Results Notes R1.1 Copyright 2015 LS Research Page 2 of 13

3 2 General Information 2.1 Summary The test results below show that the TiWi-C-W does not contain any of the 161 chemicals that are classified by REACH as Substances of Very High Concern (SVHC). 2.2 Date of Test May 13, 2015 to May 20, Test Laboratory The chemical testing was completed by SGS Taiwan LTD, an independent accredited laboratory. 2.4 Description of Sample This testing was performed on LSR part number TiWi-C-W Module 2.5 Definitions MDL = Method Detection Limit. mg/kg = ppm. N.D. = Not Detected. (The result is below the MDL.) ICP-AES = Inductively Coupled Plasma-Atomic Emission Spectrometer. UV-VIS = Ultraviolet-Visible Spectrophotometer GC-MS = Gas Chromatograph-Mass Spectrometer. LC-MS = Liquid Chromatograph mass spectrometer. GC = Gas Chromatograph FPD = Flame photometric detector GC-FID = Gas Chromatograph-flame ionization detector. LC/MS/DAD = Liquid Chromatograph-mass spectrometer-diode array detector R1.1 Copyright 2015 LS Research Page 3 of 13

4 2.6 Revision History Date ECN Change Description Revision 6/10/ /2015 Initial Release Measurement Flow Chart Table 1 Revision History Sampling Sample pretreated by acid digestion, solvent extraction Analyzed by ICP-AES, UV-VIS, GC/MS, LC/MS, GC, FPD, LC/MS/DAD Data Figure R1.1 Copyright 2015 LS Research Page 4 of 13

5 3 Chemical Analysis Results RL Concentration Classification Anthracene (CAS No ) 0.05 N. D. PBT 4,4 -Diaminodiphenylmethane (MDA) 0.05 N. D. CC 1B (CAS NO. : ) DBP (Dibutyl phthalate) (CAS No.: ) 0.05 N. D. TRC 1B BBP (Butyl Benzyl phthalate) (CAS No.: ) 0.05 N. D. TRC 1B DEHP (Bis (2-ethyl(hexyl)phthalate)) (CAS No.: ) 0.05 N. D. EQC 5-tert-butyl-2,4,6-trinitro- m-xylene (Musk Xylene) 0.05 N. D. vpvb (CAS No.: ) Hexabromocyclododecane, (HBCDD) and all major diastereoisomers 0.05 N. D. PBT identified (α- HBCDD, β- HBCDD, 7- HBCDD) (CAS No.: and ( , , )) Alkanes, C10-13, chloro (Short Chain Chlorinated Paraffins) (CAS No.: 0.05 N. D. PBT ) Bis(tributyltin)oxide (TBTO)*** (CAS No.: ) - N. D. PBT Cobalt dichloride (CAS No.: ) N. D. CC 1B; TRC 1B Diarsenic pentaoxide*** (CAS No.: ) - N. D. CC 1A Diarsenic trioxide*** (CAS No.: ) - N. D. CC 1A Triethyl arsenate*** (CAS No.: ) - N. D. CC 1A Lead hydrogen arsenate*** (CAS No.: ) - N. D. CC 1A; TRC 1A Sodium chromate*** (CAS No.: ) - N. D. CC 1B; MC 1B; TRC lb Ammonium dichromate*** (CAS No.: ) - N. D. CC 1B; MC 1B; TRC lb Potassium dichromate*** (CAS No.: ) - N. D. CC 1B; MC 1B; TRC lb Potassium chromate*** (CAS No.: ) - N. D. CC 1B; MC 1B Sodium dichromate*** (CAS No.: , (*)) - N. D. CC 1B; MC 1B; TRC lb Chromium trioxide ***(CAS No.: ) - N. D. CC 1B; MC 1B Acids generated from chromium trioxide and their oligomers: Chromic acid*** (CAS No.: ) Acids generated from chromium trioxide and their oligomers: Dichromic acid*** (CAS No.: ) Acids generated from chromium trioxide and their oligomers: Oligomers of chromic acid and dichromic acid ( *1) - N. D. CC 1B - N. D. CC 1B - N. D. CC 1B R1.1 Copyright 2015 LS Research Page 5 of 13

6 RL Concentration Classification Strontium chromate*** (CAS No.: ) - N. D. CC 1B Anthracene oil (CAS No.: ) (**) 0.05 N. D. PBT; vpvb; CC lb Anthracene oil, anthracene paste, distn. Lights (CAS No.: ) (**) 0.05 N.D. PBT; vpvb; CC lb; MC 1B Anthracene oil, anthracene paste, anthracene fraction (CAS No.: ) (**) 0.05 N. D. PBT; vpvb; CC lb; MC 1B Anthracene oil, anthracene-low (CAS No.: ) (**) 0.05 N. D. PBT; vpvb; CC 1B; MC lb Anthracene oil, anthracene paste (CAS No.: ) (**) 0.05 N. D. PBT; vpvb; CC 1B; MC lb Pitch, coal tar, high-temp. (CAS No.: ) (**) 0.05 N. D. PBT; vpvb; CC lb DIBP (Di-isobutyl phthalate) (CAS No.: ) 0.05 N. D. TRC lb 2,4-Dinitrotoluene (CAS No.: ) 0.05 N.D. CC 1B Tris(2-chloroethyl) phosphate (TCEP) (CAS No.: ) 0.05 N.D. TRC lb Lead chromate*** (CAS No.: ) (~5) - N.D. CC IB; TRC la Lead chromate molybdate sulphate red*** (C.I. Pigment Red 104) (CAS - N.D. CC lb; TRC la No.: ) (~5) Lead sulfochromate yellow*** (C.I. Pigment Yellow 34) - N.D. CC IB; TRC la (CAS No.: ) (~5) Acrylamide (CAS No.: ) 0.05 N.D. CC lb; MC 1B Boric acid*** (CAS No.: ; ) - N.D. TRC lb Disodium tetraborate, anhydrous*** (CAS No.: , , - N.D. TRC lb ) Tetraboron disodium heptaoxide, hydrate (CAS No.: ) (*2) - N.D. TRC lb Trichloroethylene (CAS No.: ) 0.05 N.D. CC 1B Cobalt(II) sulphate*** (CAS No.: ) - N/A* CC 1B; TRC lb Cobalt(II) dinitrate*** (CAS No.: ) - N/A* CC 1B; TRC lb Cobalt(II) carbonate*** (CAS No.: ) - N/A* CC 1B; TRC lb Cobalt(II) diacetate*** (CAS No.: ) - N/A* CC 1B; TRC lb 2-Methoxyethanol (CAS No.: ) 0.05 N.D. TRC 1B 2-Ethoxyethanol (CAS No.: ) 0.05 N.D. TRC 1B 2-ethoxyethyl acetate (CAS No.: ) 0.05 N.D. TRC 1B 1,2-Benzenedicarboxylic acid, di-c7-ll-branched and linear alkyl esters (DHNUP) (CAS No.: ) 0.05 N.D. TRC 1B R1.1 Copyright 2015 LS Research Page 6 of 13

7 RL Concentration Classification Hydrazine (CAS No.: ; ) 0.05 N.D. CC 1B 1-methyl-2-pyrrolidone (CAS No.: ) 0.05 N.D. TRC 1B 1,2,3-trichloropropane (CAS No.: ) 0.05 N.D. CC 1B; TRC 1B 1, 2-Benzenedicarboxylic acid, di-c6-8-branched alkyl esters, C7-rich 0.05 N.D. TRC 1B (DIHP) (CAS No.: ) Arsenic acid*** (CAS No.: ) - N.D. CC 1A Calcium arsenate*** (CAS No.: ) - N.D. CC 1A Trilead diarsenate*** (CAS No.: ) (~1) - N.D. CC 1A; TRC 1A Lead diazide, Lead azide*** (CAS No.: ) - N.D. TRC 1A Lead styphnate*** (CAS No.: ) - N.D. TRC 1A Lead dipicrate*** (CAS No.: ) - N.D. TRC 1A Dichromium tris (chromate)*** (CAS No.: ) - N.D. CC 1B Potassium hydroxyoctaoxodizincatedi-chromate*** - N.D. CC 1A (CAS No.: ) Pentazinc chromate octahydroxide*** (CAS No.: ) - N.D. CC 1A Formaldehyde, oligomeric reaction products with aniline (technical 0.05 N.D. CC 1B MDA) (CAS No.: ) Bis(2-methoxyethyl) phthalate (CAS No.: ) 0.05 N.D. TRC 1B 2-Methoxyaniline; o-anisidine (CAS No.: ) 0.05 N.D. CC 1B 4-(1,1,3,3-tetramethylbutyl) phenol, (4-tert-Octylphenol) (CAS No.: N.D. EQC 66-9) 1,2-Dichloroethane (CAS No.: ) 0.05 N.D. CC 1B Bis(2-methoxyethyl) ether (CAS No.: ) 0.05 N.D. TRC lb N,N-dimethylacetamide (DMAC) (CAS No.: ) 0.05 N.D. TRC lb 2,2'-dichloro- 4,4'- methylenedianiline (MOCA) 0.05 N.D. CC lb (CAS No.: ) Phenolphthalein (CAS No.: ) 0.05 N.D. CC lb Aluminosilicate, Refractory Ceramic Fibres [oxides of aluminium and silicon are the main components present (in the fibres) within variable concentration ranges] Zirconia Aluminosilicate, Refractory Ceramic Fibres [oxides of aluminium, silicon and zirconium are the main components present (in the fibres) within variable concentration ranges] 0.05 N.D. CC lb 0.05 N.D. CC lb R1.1 Copyright 2015 LS Research Page 7 of 13

8 RL Concentration Classification 1,2-bis (2-methoxyethoxy) ethane (TEGDME; triglyme) 0.05 N.D. TRC 1B (CAS No.: ) 1,2-dimethoxyethane; ethylene glycol dimethyl ether (EGDME) (CAS 0.05 N.D. TRC 1B No.: ) Formamide (CAS No.: ) 0.05 N.D. TRC 1B Lead (I I) bis(methanesulfonate)*** (CAS No.: ) - N.D. TRC lb TGIC (1,3,5-tris(oxiranylmethyl)- 1,3,5- triazine-2,4,6 (1H,3H,5H)-trione) 0.05 N.D. MC 1B (CAS No.: ) β TGIC (1,3,5-tris ((2S and 2R)-2,3-epoxypropyl) N.D. MC 1B 1,3,5-triazine-2,4,6- (1H,3H,5H)-trione) (CAS No.: ) (~3) 4,4 - bis (dimethylamino) benzophenone (Michler's ketone) (CAS No.: 0.05 N.D. CC 1B ) N,N,N',N'- tetramethyl- 4,4'-methylenedianiline (Michler's base) (CAS 0.05 N.D. CC 1B No.: ) (4-(4,4'-bis(dimethylamino) benzhydrylidene) cyclohexa-2,5-dien N.D. CC 1B ylidene) dimethylammonium chloride (C.I. Basic Violet 3) (CAS No.: ) (with 0.1 of Michler's ketone or Michler's base) [4-[[4-anilino-1-naphthyl) [4-(dimethylamino) phenyl] methylene] 0.05 N.D. CC 1B cyclohexa-2,5-dien-1-ylidene) dimethylammonium chloride (C.I. Basic Blue 26) (CAS No.: ) [with 0.1 of Michler's ketone or Michler's base) α,α-bis [4-(dimethylamino) phenyl]-4 (phenylamino) naphthalene N.D. CC 1B methanol (C.I. Solvent Blue 4) (CAS No.: ) [with 0.1 of Michler's ketone or Michler's base) Diboron trioxide*** (CAS No.: ) - N.D. TRC lb 4,4'-bis (dimethylamino)-4' '-(methylamine) trityl alcohol 0.05 N.D. CC 1B (CAS No.: ) [with 0.1 of Michler's ketone or Michler's base) Bis(pentabromophenyl) ether (DecaBDE) 0.05 N.D. PBT (CAS No.: ) Pentacosafluorotridecanoic acid (CAS No.: ) 0.05 N.D. PBT Tricosafluorododecanoic acid (CAS No.: ) 0.05 N.D. PBT Henicosafluoroundecanoic acid (CAS No.: ) 0.05 N.D. PBT Heptacosafluorotetradecanoic acid (CAS No.: ) 0.05 N.D. PBT 4-(1,1,3,3-tetramethylbutyl) phenol, ethoxylated- covering well-defined substances and UVCB substances, polymers and homologues 0.05 N.D. EQC R1.1 Copyright 2015 LS Research Page 8 of 13

9 4-Nonylphenol, branched and linear - substances with a linear and/or branched alkyl chain with a carbon number of 9 covalently bound in position 4 to phenol, covering also UVCB- and well-defined substances which include any of the individual isomers or a combination thereof Diazene-1,2-dicarboxamide (C,C'-azodi(formamide)) (CAS No.: ) Cyclohexane-1,2-dicarboxylic anhydride (HHPA), cis-cyclohexane-1,2- dicarboxylic anhydride, trans-cyclohexane- 1,2- dicarboxylic anhydride (Hexahydrophthalic anhydride - HHPA) (CAS No.: , , ) Hexahydromethylphathalic anhydride (CAS No.: ) Hexahydro-4-methylphathalic anhydride (CAS No.: ) Hexahydro-1-methylphathalic anhydride (CAS No.: ) Hexahydro-3-methylphathalic anhydride (CAS No.: ) RL Concentration Classification 0.05 N.D. EQC 0.05 N.D. EQC 0.05 N.D. EQC 0.05 N.D. EQC Methoxy acetic acid (CAS No.: ) 0.05 N.D. TRC 1B 1, 2-Benzenedi carboxylic acid, dipentylester, branched and linear (CAS 0.05 N.D. TRC 1B No.: ) Diisopentylphthalate (CAS No.: ) 0.05 N.D. TRC 1B N-pentyl-isopentylphtalate (CAS No.: ) 0.05 N.D. TRC 1B 1,2-Diethoxyethane (CAS No.: ) 0.05 N.D. TRC 1B N,N-dimethylformamide; dimethyl formamide 0.05 N.D. TRC 1B (CAS No.: ) Dibutyltin dichloride (DBTC) (CAS No.: ) - N.D. TRC 1B Acetic acid, lead salt, basic*** (CAS No.: ) - N.D. TRC 1A Trilead bis(carbonate) dihydroxide (basic lead carbonate)*** (CAS No.: - N.D. TRC 1A ) Lead oxide sulfate*** (CAS No.: ) - N.D. TRC 1A [Phthalato(2-)] dioxotrilead*** (CAS No.: ) - N.D. TRC 1A Dioxobis(stearato) trilead*** (CAS No.: ) - N.D. TRC 1A Fatty acids, C16-18, lead salts*** (CAS No.: ) - N.D. TRC 1A Lead cyanamidate*** (CAS No.: ) - N.D. TRC 1A Lead dinitrate*** (CAS No.: ) - N.D. TRC 1A Lead oxide (lead monoxide)*** (CAS No.: ) - N.D. TRC 1A Lead tetroxide (orange lead)*** (CAS No.: ) - N.D. TRC 1A R1.1 Copyright 2015 LS Research Page 9 of 13

10 RL Concentration Classification Pentalead tetraoxide sulphate*** (CAS No.: ) - N.D. TRC 1A Silicic acid, lead salt*** (CAS No.: ) - N.D. TRC 1A Sulfurous acid, lead salt, dibasic*** (CAS No.: ) - N.D. TRC 1A Tetraethyllead*** (CAS No.: ) - N.D. TRC 1A Tetralead trioxide sulphate (CAS No.: ) - N.D. TRC 1A Lead bis(tetrafluoroborate)*** (CAS No.: ) - N.D. TRC 1A Lead titanium trioxide*** (CAS No.: ) - N.D. TRC 1A Lead Titanium Zirconium Oxide*** (CAS No.: ) - N.D. TRC 1A Pyrochlore, antimony lead yellow*** (CAS No.: ) - N.D. TRC 1A Trilead dioxide phosphonate*** (CAS No.: ) - N.D. TRC 1A Silicic acid, barium salt, lead-doped (~4) (CAS No.: ) 0.05 N.D. TRC 1A Furan (CAS No.: ) 0.05 N.D. CC 1B Propylene oxide; 1,2-epoxypropane: methyloxirane 0.05 N.D. CC lb: MC IB (CAS No.: ) Diethyl sulphate (CAS No.: ) 0.05 N.D. CC 1B; MC IB Dimethyl sulphate (CAS No.: ) 0.05 N.D. CC lb 3-ethyl-2-methyl-2- (3-methylbutyl)-1,3-oxazolidine 0.05 N.D. TRC lb (CAS No.: ) Dinoseb (CAS No.: ) 0.05 N.D. TRC lb 4,4'-methylenedi-o-toluidine (CAS No.: ) 0.05 N.D. CC 1B 4,4'-oxydianiline and its salts (CAS No.: ) 0.05 N.D. CC 1B; MC IB 4-Aminoazobenzene; 4-Phenylazoaniline (CAS No.: ) 0.05 N.D. CC 1B 4-methyl-m-phenylenediamine (2,4-toluenediamine) 0.05 N.D. CC 1B (CAS No.: ) 6-methoxy-m-toluidine (p-cresidine) (CAS No.: ) 0.05 N.D. CC 1B Biphenyl-4-ylamine (CAS No.: ) 0.05 N.D. CC 1A o-aminoazotoluene (CAS No.: ) 0.05 N.D. CC 1B o-toluidine; 2-Aminotoluene (CAS No.: ) 0.05 N.D. CC 1B N-methylacetamide (CAS No.: ) 0.05 N.D. TRC 1B R1.1 Copyright 2015 LS Research Page 10 of 13

11 RL Concentration Classification 1-bromopropane (CAS No.: ) 0.05 N.D. TRC 1B Pentadecafluorooctanoic acid (PFOA) 0.05 N.D. TRC 1B & PBT (CAS No.: ) Ammoniumpentadecafluorooctanoate (APFO)*** - N.D. TRC 1B & PBT (CAS No.: ) Cadmium (Cd) (CAS No.: ) N.D. CC lb & EQC Cadmium oxide*** (CAS No.: ) - N.D. CC lb & EQC DPP (Di -pentyl phthalate) (CAS No.: ) 0.05 N.D. TRC 1B 4-Nonylphenol, branched and linear, ethoxylated (substances with a 0.05 N.D. EQC linear and/or branched alkyl chain with a carbon number of 9 covalently bound in position 4 to phenol, ethoxylated covering UVCBand well-defined substances, polymers and homologues, which include any of the individual isomers and/or combinations thereof) Dihexyl phthalate (CAS No.: ) 0.05 N.D. TRC 1B Disodium 3,3'-((1,1'-biphenyl)-4,4'-diylbis(azo))bis( N.D. CC lb aminonaphthalene-1-sulphonate) (C.I. Direct Red 28) (CAS No.: ) Disodium 4-amino-3-((4'-((2,4-diaminophenyl)azo)(1,1'-biphenyl) N.D. CC lb yl)azo) -5-hydroxy-6-(phenylazo)naphthalene-2,7-disulphonate (C.I. Direct Black 38) (CAS No.: ) lmidazol idine-2-thione; 2-imidazoline-2-thiol 0.05 N.D. TRC lb (CAS No.: ) Trixylyl phosphate (CAS No.: ) 0.05 N.D. TRC lb Cadmium sulphide*** (CAS No.: ) - N.D. CC IB & EQC Lead di(acetate)*** (CAS No.: ) - N.D. TRC la 1, 2-Benzenedicarboxylic acid, dihexyl ester, branched and linear (CAS 0.05 N.D. TRC lb No.: ) Cadmium chloride*** (CAS No.: ) - N.D. CC 1B; MC 1B; TRC 1B; EQC Sodium perborate; perboric acid, sodium salt*** - N.D. TRC lb Sodium peroxometaborate*** (CAS No.: ) - N.D. TRC lb 2-(2H-benzotriazol-2-yl)-4,6-ditertpentylphenol (UV-328) (CAS No.: 0.05 N.D. vpvb & PBT ) 2-benzotriazol-2-yl-4,6-di-tert-butylphenol (UV-320) 0.05 N.D. vpvb & PBT (CAS No.: ) Cadmium fluoride*** (CAS No.: ) - N.D. CC 1B; MC 1B; TRC 1B; EQC R1.1 Copyright 2015 LS Research Page 11 of 13

12 RL Concentration Classification Cadmium sulphate*** (CAS No.: ; ) - N.D. CC 1B; MC 1B; TRC 1B; EQC 2-ethylhexyl 10-ethyl-4,4-dioctyl-7-oxo-8-oxa-3,5-dithia-4- - N.D. TRC lb stannatetradecanoate (DOTE)*** (CAS No.: ) Reaction mass of 2-ethylhexyl 10-ethyl-4,4-dioctyl-7-oxo-8-oxa-3,5- dithia-4-stannatetradecanoate and 2-ethylhexyl 10-ethyl-4-((2-((2- ethylhexyl)oxy)-2-oxoethyl)thio)-4- octyl-7-oxo-8-oxa-3,5-dithia-4-stannatetradecanoate (reaction mass of DOTE and MOTE)*** - N.D. TRC lb 3.1 Notes 1. mglkg = ppm ; 0.l wt = 1000 ppm 2. N.D. = not detected = below Reporting Limit 3. RL = Reporting Limit 4. "-" = Not Regulated 5. (*): (CAS No.: ) = X (conc. of Sodium dichromate dihydrate = cone. of sodium dichromate X ) 6. (**):The concentrations of above mentioned mixtures are evaluated per the gained composition rate between the selected marks and the mixtures. 7. (*1): Oligomers of chromic acid and dichromic acid : since the oligomers are made of the unknown amount of chromic acid or dichromic acid that results in no fixed molecular weight, therefore the monomer of chromic acid or dichromic acid is relevant and considered. 8. (*2): Tetraboron disodium heptaoxide, hydrate: Only anhydrous form of disodium tetraborate is relevant and considered according to ECHA explanation (Ref no.: INC ). 9. (***): The substance was calculated by the test results of MonooctylTin, Dioctyl Tin, Tributyl Tin, PFOA or element (Ex. Arsenic, Lead, Cr(VI), Boron, Cobalt, Barium, Cadmium respectively). The test result is given as: RL Concentration Tributyl Tin (TBT) 0.05 N. D. Arsenic (As) (~2) N. D. Lead (Pb) N.D. Hexavalent Chromium Cr(VI) N.D R1.1 Copyright 2015 LS Research Page 12 of 13

13 RL Concentration Boron (B) (~2) N.D. Cobalt (Co) Dioctyl Tin (DOT) N.D. MonooctylTin (MOT) N.D. Dbutyl Tin (DBT) 0.05 N.D. 10. (~1): Regarding the compound containing arsenic and lead, lead and arsenic are tested and respectively used for the calculation of the independent concentration of the compound containing arsenic and lead. The minimum value of the two independently calculated concentrations is used as the final concentration for the report. 11. (~2): The extracted soluble Boron I Arsenic are detected by ICP-AES. 12. (~3): TGIC is a mixture and also contains β-tgic. According to the ECHA's technical dossier the ratio of β-tgic to TGIC is around 1 to 10. Therefore β-tgic is issued based on the above-mentioned ratio. 13. (~4): Only if both qualitative results of lead and silicon are positive, the test result of the compound will be calculated based on the concentration of barium. 14. (~5): Regarding the compound containing Cr(VI) and lead, lead and Cr(VI) are tested and respectively used for the calculation of the independent concentration of the compound containing Cr(VI) and lead. The minimum value of the two independently calculated concentrations is used as the final concentration for the report. 15. N/A*: Not Applicable to direct analysis. The item can't directly be identified. Therefore the specific element(s) of SVHC was analyzed according to the recommendation from the ECHA. The submitted sample was found to contain detectable amount of specific element(s) of SVHC. Upon further test verification or information provided from the client, the source of the detectable specific element(s) can't be identified from SVHC. Therefore the test result is expressed as N/A*. 16. CC 1A: Carcinogen Category 1A 17. CC 1B: Carcinogen Category 1B 18. MC 1A: Mutagen Category 1A 19. MC 1B: Mutagen Category 1B 20. PBT & vpvb: Persistent, Bio accumulative and Toxic or very Persistent and very Bio accumulative 21. EQC: Equivalent concern 22. TRC 1A: Toxic to Reproduction Category 1A 23. TRC 1B: Toxic to Reproduction Category 1B R1.1 Copyright 2015 LS Research Page 13 of 13

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