TEST REPORT. Serie : Receiving Date: 06/07/2017 Test Start Date: 08/07/2017 Test End Date: *SUMMARY OF TEST CONCLUSIONS
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1 Address: Attn: Client: Tel:+ Fax: + Code: The following sample was (were) submitted and identified by the client as: Sample description: RAW MATERIAL Batch No.: Job no Report No.: Reference No.: NARANJA FELPA Composition indicated: UNKNOWN Serie : Receiving Date: 06/07/2017 Test Start Date: 08/07/2017 Test End Date: 19/07/2017 SOP description s * SOP 25 - Colour fastness to artificial light for fabrics - Xenom lamp * SOP 52-Determination of arylamines for natural samples * SOP 52-Determination of arylamines for synthetic samples SOP 58-Determination of formaldehyde by photometric in textile samples (DC) * SOP 70-Determination of allergenous dyes SOP 55-Determination of cadmium and lead in textile samples by ICP-MS * SOP 20-Determination of the content of phenols SOP 60-Colour Fastness to Rubbing (Direct Contact) SOP 62-Colour Fastness to Acid perspiration (Direct contact) SOP 62-Colour Fastness to Alkaline perspiration (Direct contact) SOP 13 - Colour fastness to domestic washing C06 *SUMMARY OF TEST CONCLUSIONS Sample Tested Pag. 1 of 11
2 * 250 SOP 25 - Colour fastness to artificial light for fabrics - Xenom lamp 5 S S Colour change Blue Scale 7 Hours test process 30 - Applied standard based in UNE-EN ISO 105-B02:2001 (Equivalent to ISO 105-B02:1994) - NA = not applicable Note 1: Used Blue scale from 1 to 8. * 520 SOP 52-Determination of arylamines for natural samples Composite Sample S (N = 6) 6 S S dianisidine (3,3-dimethoxybenzidine) n.d. 2,4,5-trimethylaniline n.d. 2,4-Diaminotoluene n.d. 2,4-dimethylaniline n.d. 2,6-dimethylaniline n.d. 2-Nafthylamine n.d. 3,3-dichlorobenzidine n.d. 3,3-dimethylbenzidine n.d. 4,4-Diaminediphenyl sulfide n.d. 4,4-Oxydianiline n.d. 4,4-diaminophenylmethane n.d. 4,4-methylen-bis-(2-Chloroaniline) n.d. 4,4-methylendi-o-toluidine n.d. 4-Aminoazobenzene n.d. Pag. 2 of 11
3 S Aminobiphenyl n.d. 4-Chloro-o-toluidine n.d. 4-Chloroaniline n.d. 4-Methoxy-m-phenilenediamine n.d. 5-Nitro-o-toluidine n.d. 6-methoxy-m-toluidine n.d. Benzidine n.d. o-aminoazotoluene n.d. o-anisidine n.d. o-toluidine n.d. - Applied standard UNE-EN : Requirement by the client= 20 mg Kg-1 for textile 30 mg Kg-1 for leather goods - (Nº=..) = number of subsamples included. If N>number of subsamples visible, in this composite sample it mixed different references by customer indications. Report Unit: mg Kg-1 n.d.= not detected (<MDL) MDL (Method Detection Limit )= 1,0 mg Kg-1 * 522 SOP 52-Determination of arylamines for synthetic samples Composite Sample S (N = 5) 7 S S dianisidine (3,3-dimethoxybenzidine) n.d. 2,4,5-trimethylaniline n.d. 2,4-Diaminotoluene n.d. 2,4-dimethylaniline n.d. 2,6-dimethylaniline n.d. 2-Nafthylamine n.d. Pag. 3 of 11
4 S ,3-dichlorobenzidine n.d. 3,3-dimethylbenzidine n.d. 4,4-Diaminediphenyl sulfide n.d. 4,4-Oxydianiline n.d. 4,4-diaminophenylmethane n.d. 4,4-methylen-bis-(2-Chloroaniline) n.d. 4,4-methylendi-o-toluidine n.d. 4-Aminoazobenzene n.d. 4-Aminobiphenyl n.d. 4-Chloro-o-toluidine n.d. 4-Chloroaniline n.d. 4-Methoxy-m-phenilenediamine n.d. 5-Nitro-o-toluidine n.d. 6-methoxy-m-toluidine n.d. Benzidine n.d. o-aminoazotoluene n.d. o-anisidine n.d. o-toluidine n.d. - Applied standard UNE-EN : Requirement by the client= 20 mg Kg-1 for textile 30 mg Kg-1 for leather goods - (Nº=..) = number of subsamples included. If N>number of subsamples visible, in this composite sample it mixed different references by customer indications. Report Unit: mg Kg-1 n.d.= not detected (<MDL) MDL (Method Detection Limit )= 1,0 mg Kg SOP 58-Determination of formaldehyde by photometric in textile samples (DC) Composite Sample S (N = 6) 8 S Pag. 4 of 11
5 Formaldehyde S Applied standard ITX-GB/T / Requirement by the client, products for over 3 years= 75 mg Kg-1 for items of direct contact 300 mg Kg-1 garment with indirect contact - (Nº=..) = number of subsamples included. If N>number of subsamples visible, in this composite sample it mixed different references by customer indications. Report Unit: mg Kg-1 n.d.= not detected = <LOQ LOQ (Limit of quantification )= 2,0 mg Kg-1 * 700 SOP 70-Determination of allergenous dyes 9 S S Disperse Blue n.d. Disperse Blue n.d. Disperse Blue n.d. Disperse Blue n.d. Disperse Blue n.d. Disperse Blue n.d. Disperse Blue n.d. Disperse Blue n.d. Disperse Brown n.d. Disperse Orange n.d. Disperse Orange n.d. Pag. 5 of 11
6 S Disperse Orange n.d. Disperse Red n.d. Disperse Red n.d. Disperse Red n.d. Disperse Yellow n.d. Disperse Yellow n.d. Disperse Yellow n.d. Disperse Yellow n.d. Disperse Yellow n.d. - Applied standard DIN Requirement by the client= 50,0 mg Kg-1 Report Unit: mg Kg-1 n.d.= not detected (<MDL) MDL (Method Detection Limit )= 1,0 mg Kg SOP 55-Determination of cadmium and lead in textile samples by ICP-MS Composite Sample S (N = 4) 11 S S Cadmium n.d. Lead n.d. - Applied standard CPSC-CH-E (2012) - Requirement by the client, products for over 3 years= 75,0 mg Kg-1 for cadmium 100,0 mg Kg-1 for lead Pag. 6 of 11
7 Report Unit: mg Kg-1 n.d.= not detected = <LOQ LOQ (Limit of quantification )= 50,0 mg Kg-1 * 200 SOP 20-Determination of the content of phenols 10 S S PCP n.d. TeCP n.d. - Requirement by the client= 0,05 mg Kg-1. Report Unit mg Kg-1 n.d= not detected (<MDL) MDL (Method Detection Limit )= 0,05 mg Kg SOP 60-Colour Fastness to Rubbing (Direct Contact) 1 S S Cross Staining Length direction Dry Colour Change 5 Length direction Dry Staining 3 Length direction Wet Colour Change 4/5 Length direction Wet Staining 2 (**) Width direction Dry Colour Change 4/5 Width direction Dry Staining 2/3 (**) Width direction Wet Colour Change 4/5 Width direction Wet Staining 2 (**) Pag. 7 of 11
8 - Applied standard UNE-EN ISO 105-X12:2016 (Equivalent to ISO 105-X12:2016) - Requirement by the client, products for over 3 years= 3 in Grey Scale ISO 105-A02 for Colour Change 3 in Grey Scale ISO 105-A03 for Colour Staining. - Requirement by the client, products intended for children under 3 years= 4 in Grey Scale ISO 105-A02 for Colour Change 4 in Grey Scale ISO 105-A03 for Colour Staining. - = not applicable Note 1: Rubbing plug with a cylinder of (16 ± 0.1) mm, which apply a downward force of (9 ± 0.2) N Note 2: Only for Hair fabrics: Rubbing plug with a rectangular area of 19 mm x 25.4 mm, which apply a downward force of (9 ± 0.2) N Note 3: Adjacent Fabric Monofibre used: Cotton Note 4: Impregnation/absorption percentage for wet rubbing: % Note 5: Conditioning time for analyzed fabrics and adjacent fabrics: 4 hours Note 6: Environmental conditions: (20±2) ºC and (65±2) % of RH 621 SOP 62-Colour Fastness to Acid perspiration (Direct contact) 2 S S Colour Change 5 Cross Staining Staining Acetate 5 Staining Acrylic 5 Staining Cotton 5 Staining Linen Staining Polyamide 5 Staining Polyester 5 Staining Silk Staining Viscose Staining Wool 5 - Applied standard UNE-EN ISO 105-E04:2013 (Equivalent to ISO 105-E04:2013) - Requirement by the client, products for over 3 years= 3 in Grey Scale ISO 105-A02 for Colour Change 3 in Grey Scale ISO 105-A03 for Colour Staining. - Requirement by the client, products intended for children under 3 years= 3-4 in Grey Scale ISO 105-A02 for Colour Change 3-4 in Grey Scale ISO 105-A03 for Colour Staining. - = not applicable Pag. 8 of 11
9 Note 1: Acid solution used with ph 5.5 (± 0.2) Note 2: Adjacent Fabric Monofibre used: if only appear two results in staining Note 3: Adjacent Fabric Multifibre type used: DW, see results if appear more than two results in staining. Note 4: Perspirometer position for test: Vertical 622 SOP 62-Colour Fastness to Alkaline perspiration (Direct contact) 3 S S Colour Change 5 Cross Staining Staining Acetate 5 Staining Acrylic 5 Staining Cotton 5 Staining Linen Staining Polyamide 5 Staining Polyester 5 Staining Silk Staining Viscose Staining Wool 5 - Applied standard UNE-EN ISO 105-E04:2013 (Equivalent to ISO 105-E04:2013) - Requirement by the client, products for over 3 years= 3 in Grey Scale ISO 105-A02 for Colour Change 3 in Grey Scale ISO 105-A03 for Colour Staining. - Requirement by the client, products intended for children under 3 years= 3-4 in Grey Scale ISO 105-A02 for Colour Change 3-4 in Grey Scale ISO 105-A03 for Colour Staining. - = not applicable Note 1: Alkaline solution used with ph 8 (± 0.2) Note 2: Adjacent Fabric Monofibre used: if only appear two results in staining Note 3: Adjacent Fabric Multifibre type used: DW, see results if appear more than two results in staining. Note 4: Perspirometer position for test: Vertical Pag. 9 of 11
10 130 SOP 13 - Colour fastness to domestic washing C06 4 S S Colour Change 5 Cross Staining Staining Acetate 5 Staining Acrylic 5 Staining Cotton 5 Staining Linen Staining Polyamide 5 Staining Polyester 5 Staining Silk Staining Viscose Staining Wool 5 Washing Temperature 30ºC - Applied standard UNE-EN ISO 105-C06:2010 (Equivalent to ISO 105-C06:2010) - = not applicable - Requirement recommended= 3 in Grey Scale ISO 105-A02 for Colour Change 3 in Grey Scale ISO 105-A03 for Colour Staining. Note 1: Test Temperature: Indicated in results table Note 2: Test number according with Tª: A1S (40ºC - 30 min) / A1M (40ºC - 45 min) / B1S (50ºC - 30 min) / B1M (50ºC - 45 min) / C1S (60 ºC - 30 min) / C1M (60 ºC - 40 min) Note 3: Steel balls used: Yes Note 4: Treatment with acetic acid: No Note 5: Detergent used: ECE phosphate reference detergent (B) Note 6: Adjacent Fabric Monofibre used: if only appear two results in staining Note 7: Adjacent Fabric Multifibre type used: DW, see results if appear more than two results in staining. Pag. 10 of 11
11 TEST REPORT Date: 19/07/2017 Issue Signed: Manuel Lolo Signed: Pablo Perez General Manager Chemical Lab Manager Signed: Esteban Ramirez Physical Lab Manager Pag. 11 of 11
TEST REPORT. Serie : Receiving Date: 06/07/2017 Test Start Date: 08/07/2017 Test End Date: *SUMMARY OF TEST CONCLUSIONS
Address: Attn: Tel: Client: e-mail: Code: The following sample was (were) submitted and identified by the client as: Sample description: RAW MATERIAL Batch No.: Job no Report No.: 17-010610 Reference No.:
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