ENREGISTREMENT DES BULLETINS ANALYTIQUES : CHROMATOGRAPHIE ESSENTIAL OIL CHROMATOGRAPHY SHEET RECORDS

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FORM-LAB005-B Page 1 sur 7 Date : 04/08/2011 Huile essentielle de / Essential oil of : Helichryse sauvage / Helichrysum Italian Numéro de lot / Lot Number : FLE043F230611F Densité à 20 C (g/cm 3 ) / Density to 20 C (g/cm 3 ) : nd Indice de réfraction / Refractive index : nd Pouvoir rotatoire à 20 C / Optical rotation to 20 C : nd Mode de culture / Culture mode : Sauvage / Wild Pays / Country : France Année de production / Production year : 2011 Mode d extraction / Extraction mode : Distillation à la vapeur / Steam distillation % Bio / % Organic : 100% Bio / 100% Organic Nom Latin / Latin Name : Helichrysum italicum Parties utilisées / Used Parts : Sommités Fleuris / Flowering Top Hydocarbures alcools cétones aldéhyde hydrocarbures sesquiterpéniques

FORM-LAB005-B Page 2 sur 7 3-methyl-cyclohexanone 0,340 nonane 0,020 ester aliphatique 0,030 methaxrylate de methyle 0,03 ester methacryllique 0,090 terpinolene isomere + cetone aliphatique 0,130 2-methyl-3-pentanone 0,210 alpha pinène 2,500 alpha-thuyene 0,020 alpha-fenchene 0,470 camphene 0,200 4-methyl-3-hexanone 0,420 beta-pinene 0,880 sabinene 0,010 beta myrcene 0,110 alpha phellandrene 0,040 isovalerate d'isobutyle 0,04 alpha terpinene 0,26 ester aliphatique 0,030 limonene 5,340 cis-arbusculone 0,050 1,8-cineole 0,85 beta-phellandrene 0,050 2-pentyl furane 0,010

FORM-LAB005-B Page 3 sur 7 cis-beta-ocimene 0,020 trans-arbusculone 0,030 gamma terpinene + trans beta ocimene 1,080 para cymene 0,270 2 methyl butyrate de 2 methylbutyle 0,090 terpinolene 0,220 angelate d'isobutyle 0,200 isovalerate d'isoamyle 0,020 acetate de cis-3-hexenyle 0,020 6 methyl -5-heptene -2-one 0,030 compose Mw=164 0,030 angelate d'alkyle 0,020 2-nonanone 0,360 angelate d'isoamyle 0,480 methyl-p-cresol 0,140 6-methyl 5 hepten-2 ol 0,030 angelate d'hexyle 0,100 composé aliphatique 0,020 cetone artemisique 0,200 2-decanone 0,030 alpha-copaene 0,030 isoitalicene 0,570 2-nonalol 0,080 trimethyl hexane dione Mw=156 0,330

FORM-LAB005-B Page 4 sur 7 linalol 1,820 italicene 2,110 alpha-cis-bergamotene 0,500 italicene isomere 0,070 fenchol 0,050 alpha-trans-bergamotene 0,280 beta-cubebene+2-undecanone 0,220 3,5-dimethyloctane-4,6-dione 0,800 terpinen-4-ol 0,890 beta-caryophyllene 0,130 cis paramenth-2-en-1-ol 0,030 gurjunene isomere 0,030 composé aliphatique 0,040 E-beta-farnesene 0,190 trans-pinocarveol 0,040 zonarène 0,050 sesquiterpene 0,030 cetone aliphatique 0,020 alpha humulene 0,040 gamma selinene 0,26 curcumene isomere 0,25 z-beta-farnesene 0,090 gamma curcumene 11,470 alpha terpineol 0,300

FORM-LAB005-B Page 5 sur 7 borneol 0,11 ester angelique 0,090 eremophilene 0,03 germacrene D 0,040 acetate de neryle 33,240 beta-bisabolene 0,150 beta selinene 0,080 alpha selinene 0,060 beta curcumene 0,370 trans pipéritol 0,020 acetate de geranyle 0,140 farnesene isomere 0,070 delta cadinene 0,020 gamma-cadinene 0,020 alpha-bisabolene 0,060 alpha-curcumene 2,470 propionate de neryle 4,760 para-methylacetophenone 0,020 nerol 3,300 butyrate de neryle 0,020 trans-carveol + ester terpenique 0,180 geraniol 0,060 composé Mw=220 0,080 methylbutyrate de neryle 0,230

FORM-LAB005-B Page 6 sur 7 composé Mw=220 0,030 isovalerate de neryle 0,330 dehydrocurcumene Mw=200 0,040 italidione I Mw=210 7,060 italidione II Mw=224 3,140 italidione isomere 0,130 composé aromatique 0,050 italidone III Mw=238 1,690 valerate de neryle 0,200 oxyde de caryophyllene 0,030 ester aliphatique 0,050 nerolidol + dione aliphatique 0,210 tiglate de neryle 0,050 guaiol 0,750 dione aliphatique 0,230 eudesma-ol isomere 0,070 sesquiterpenol Mw=222 0,200 eudesma-5-en-11-alpha-ol 1,320 sesquiterpenol 0,070 compose methoxyaromatique 0,070 eudesmol isomere 0,540 gamma eudesmol 0,220 dehydroviriflorol 0,050 guaiol isomere 0,040

FORM-LAB005-B Page 7 sur 7 sesquiterpenol 0,040 guaiol isomere 0,130 bulnesol 0,220 alpha-eudesmol 0,290 beta eudesmol 0,440 acetate de farnesyle 0,040 acide caprique 0,080 composé aliphatique 0,040 sesquiterpenol 0,040 sesquiterpenol 0,040 dione aliphatique 0,030 dione aliphatique 0,030 dione aliphatique 0,070 dione aliphatique 0,010 dione aliphatique 0,020