CERTIFICATE OF ANALYSIS - GC PROFILING

Date : April 25, 2018 CERTIFICATE OF ANALYSIS - GC PROFILING SAMPLE IDENTIFICATION Internal code : 18D18-HBN4-1-CC Customer identification : Tea Tree Oil - 10519716 Type : Essential oil Source : Melaleuca alternifolia ct. Terpinen-4-ol Customer : Health & Beauty Natural Oils ANALYSIS Method: PC-PA-014-17J19 - Analysis of the composition of an essential oil, or other volatile liquid, by FAST GC-FID (in French); identifications validated by GC-MS. Analyst : Sylvain Mercier, M. Sc., Chimiste Analysis date : April 20, 2018 Checked and approved by : Alexis St-Gelais, M. Sc., chimiste 2013-174 Note: This report may not be published, including online, without the written consent from Laboratoire PhytoChemia. This report is digitally signed, it is only considered valid if the digital signature is intact. Page 1/12

PHYSICOCHEMICAL DATA Physical aspect: Clear liquid Refractive index: 1.4778 ± 0.0003 (20 C) COMPLIANCE WITH ISO 4730:2017 (OIL OF MELALEUCA, TERPINEN-4-OL TYPE (TEA TREE OIL)) Compound Prescribed content Min. % Max. % Observed % Complies? α-pinene 1 4 2.5 Yes Sabinene tr 3.5 0.3 Yes α-terpinene 6 12 9.2 Yes Limonene 0.5 1.5 0.8 Yes para-cymene 0.5 8 2.6 Yes 1,8-Cineole tr 10 1.7 Yes γ-terpinene 14 28 19.6 Yes Terpinolene 1.5 5 3.3 Yes Terpinen-4-ol 35 48 39.1 Yes α-terpineol 2 5 2.9 Yes Aromadendrene 0.2 3 1.3 Yes Viridiflorene 0.1 3 1.1 Yes δ-cadinene 0.2 3 1.7 Yes Globulol tr 1 0.4 Yes Viridiflorol tr 1 0.2 Yes Refractive index 1.475 1.482 1.4778 Yes CONCLUSION No adulterant, contaminant or diluent has been detected using this method. The oil complies with the ISO standard for tea tree oil. Page 2/12

ANALYSIS SUMMARY Identification DB-5 (%) DB-WAX (%) Classe Ethanol 0.14 0.16 Aliphatic alcohol Isobutyral 0.04 0.05 Aliphatic aldehyde Ethyl acetate 0.01 tr Aliphatic ester Isobutanol tr 0.70* Aliphatic alcohol Isovaleral tr tr Aliphatic aldehyde 2-Methylbutyral 0.03 0.03 Aliphatic aldehyde Isoamyl alcohol tr tr* Aliphatic alcohol 2-Methylbutanol tr [tr]* Aliphatic alcohol Isobutyric acid tr Aliphatic acid (3Z)-Hexenol 0.05 0.06 Aliphatic alcohol Hexanol tr 0.01 Aliphatic alcohol α-thujene 0.91 0.91 Monoterpene α-pinene 2.48 2.47 Monoterpene Camphene 0.02* 0.01 Monoterpene α-fenchene [0.02]* tr Monoterpene Thuja-2,4(10)-diene tr 0.27* Monoterpene Sabinene 0.97* [0.27]* Monoterpene β-pinene [0.97]* [0.70]* Monoterpene 3-Methyl-3-cyclohexenone? 0.02 0.02* Aliphatic ketone Myrcene 0.83 0.84 Monoterpene Pseudolimonene 0.51* 0.01 Monoterpene α-phellandrene [0.51]* 0.51 Monoterpene (3Z)-Hexenyl acetate 0.01 0.01 Aliphatic ester α-terpinene 9.23 9.26 Monoterpene Carvomenthene 0.01 0.01 Aliphatic alcohol para-cymene 2.61 2.60 Monoterpene β-phellandrene 3.57* 1.00 Monoterpene Limonene [3.57]* 0.80 Monoterpene 1,8-Cineole [3.57] 1.72 Monoterpenic ether (Z)-β-Ocimene 0.01 19.67* Monoterpene (E)-β-Ocimene 0.02 0.02 Monoterpene γ-terpinene 19.61 [19.67]* Monoterpene cis-sabinene hydrate 0.02 0.02 Monoterpenic alcohol Terpinolene 3.34 3.30 Monoterpene trans-sabinene hydrate 0.03 0.03 Monoterpenic alcohol Linalool 0.06 0.08 Monoterpenic alcohol Unknown 0.02 1.33* Monoterpenic alcohol para-mentha-1,3,8-triene 0.01 [0.02]* Monoterpene cis-para-menth-2-en-1-ol 0.27 0.28 Monoterpenic alcohol 4-Hydroxy-4-methylcyclohex-2-enone 0.02 0.02 Aliphatic alcohol Cosmene isomer I 0.18* 0.06 Monoterpene trans-para-menth-2-en-1-ol [0.18]* 0.80* Monoterpenic alcohol Unknown 0.10 0.16* Unknown Borneol 0.01 3.03* Monoterpenic alcohol δ-terpineol tr 0.01 Monoterpenic alcohol Terpinen-4-ol 39.24* 39.12* Monoterpenic alcohol Dill ether [39.24]* tr Monoterpenic ether para-cymen-8-ol [39.24] 0.05 Monoterpenic alcohol Page 3/12

α-terpineol 2.91 [3.03]* Monoterpenic alcohol cis-piperitol 0.07 0.13 Monoterpenic alcohol Unknown 0.02 Oxygenated monoterpene trans-piperitol 0.10 1.82 Monoterpenic alcohol endo-fenchyl acetate 0.01 [0.16]* Monoterpenic ester exo-2-hydroxycineole 0.02 0.02 Monoterpenic alcohol Nerol 0.03 0.04 Monoterpenic alcohol Piperitone 0.07 0.15 Monoterpenic ketone cis-carvenone oxide? 0.02 Monoterpenic ketone trans-ascaridole glycol 0.05 0.04 Monoterpenic alcohol cis-ascaridole glycol? 0.03 0.04 Monoterpenic alcohol Thymol 0.01 0.01 Monoterpenic alcohol Carvacrol 0.01 0.01 Monoterpenic alcohol Unknown 0.03 0.03 Monoterpenic alcohol Bicycloelemene 0.03 0.02 Sesquiterpene α-cubebene 0.07 0.07 Sesquiterpene Isoledene 0.07 [0.16]* Sesquiterpene α-copaene 0.13 0.13 Sesquiterpene 7-Cubebene 0.07* 0.07 Sesquiterpene 7-Cubebene epimer? [0.07]* 0.03 Aliphatic alcohol β-cubebene 0.03 0.05 Sesquiterpene β-elemene 0.04 [1.33]* Sesquiterpene α-gurjunene 0.46 0.43 Sesquiterpene β-maaliene 0.01 0.01 Sesquiterpene β-caryophyllene 0.44 0.43 Sesquiterpene γ-maaliene 0.08 0.10 Sesquiterpene β-gurjunene 0.02 0.03 Sesquiterpene α-maaliene 0.08 [39.12]* Sesquiterpene Aromadendrene 1.40 [1.33]* Sesquiterpene Selina-5,11-diene 0.18 0.23 Sesquiterpene trans-muurola-3,5-diene 0.15 0.14 Sesquiterpene α-humulene 0.10 0.10 Sesquiterpene allo-aromadendrene 0.64* [0.80]* Sesquiterpene Valerena-4,7(11)-diene [0.64]* 0.02 Sesquiterpene γ-gurjunene 0.06 0.08 Sesquiterpene trans-cadina-1(6),4-diene 0.39* 0.35 Sesquiterpene Selina-4,11-diene [0.39]* 0.03 Sesquiterpene γ-muurolene 0.04 0.05 Sesquiterpene β-selinene 0.12 0.13 Sesquiterpene allo-aromadendr-9-ene 0.12 0.10 Sesquiterpene trans-muurola-4(15),5-diene 0.10 [3.03]* Sesquiterpene δ-selinene 0.13 1.20* Sesquiterpene Viridiflorene 2.13* [1.20]* Sesquiterpene Bicyclogermacrene [2.13]* 0.95 Sesquiterpene α-selinene [2.13]* 0.03 Sesquiterpene α-muurolene 0.19 0.16 Sesquiterpene γ-cadinene 0.04 [1.82]* Sesquiterpene trans-calamenene 0.11 0.13 Sesquiterpene Zonarene 1.74* [1.82]* Sesquiterpene δ-cadinene [1.74]* [1.82]* Sesquiterpene trans-cadina-1,4-diene 0.23 0.25 Sesquiterpene α-calacorene 0.02 0.03 Sesquiterpene Page 4/12

Eudesma-5,7(11)-diene 0.02 0.03 Sesquiterpene Unknown 0.13 0.12 Oxygenated sesquiterpene Spathulenol 0.10 0.11 Sesquiterpenic alcohol Globulol 0.40 0.38 Sesquiterpenic alcohol Gleenol 0.04 0.04 Sesquiterpenic alcohol Viridiflorol 0.19 0.19 Sesquiterpenic alcohol Cubeban-11-ol 0.16 0.26* Sesquiterpenic alcohol Ledol 0.15* 0.06 Sesquiterpenic alcohol Eudesm-5-en-11-ol analog [0.15]* 0.09 Sesquiterpenic alcohol 10-epi-Cubenol 0.01 Sesquiterpenic alcohol Rosifoliol 0.15 0.16 Sesquiterpenic alcohol 1-epi-Cubenol 0.22 0.24 Sesquiterpenic alcohol Isospathulenol 0.05 0.05 Sesquiterpenic alcohol Cubenol 0.13 [0.26]* Sesquiterpenic alcohol α-muurolol 0.05 0.06 Sesquiterpenic alcohol Total identified 98.72% 98.73% *: Two or more compounds are coeluting on this column [xx]: Duplicate percentage due to coelutions, not taken account in the identified total tr: The compound has been detected below 0.005% of total signal. Note: no correction factor was applied Page 5/12

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FULL ANALYSIS DATA Identification Column DB-5 Column DB-WAX R.T R.I % R.T R.I % Ethanol 0.35 495 0.14 0.88 909 0.16 Isobutyral 0.42 542 0.04 0.51 770 0.05 Ethyl acetate 0.50 609 0.01 0.72 863 tr Isobutanol 0.54 620 tr 2.13* 1070 0.70 Isovaleral 0.59 640 tr 0.78 888 tr 2-Methylbutyral 0.62 649 0.03 0.76 881 0.03 Isoamyl alcohol 0.95 728 tr 3.45* 1175 tr 2-Methylbutanol 0.97 730 tr 3.45* 1175 [tr] Isobutyric acid 1.13 755 tr (3Z)-Hexenol 2.04 852 0.05 5.87 1352 0.06 Hexanol 2.24 869 tr 5.50 1326 0.01 α-thujene 2.93 922 0.91 1.45 1003 0.91 α-pinene 3.00 927 2.48 1.39 995 2.47 Camphene 3.19* 940 0.02 1.73 1031 0.01 α-fenchene 3.19* 940 [0.02] 1.66 1024 tr Thuja-2,4(10)- diene 3.29 947 tr 2.31* 1088 0.27 Sabinene 3.61* 968 0.97 2.31* 1088 [0.27] β-pinene 3.61* 968 [0.97] 2.13* 1070 [0.70] 3-Methyl-3- cyclohexenone? 3.76 979 0.02 6.19* 1375 0.02 Myrcene 3.92 990 0.83 2.92 1136 0.84 Pseudolimonene 4.06* 999 0.51 2.86 1132 0.01 α-phellandrene 4.06* 999 [0.51] 2.82 1129 0.51 (3Z)-Hexenyl acetate 4.20 1008 0.01 5.10 1285 0.01 α-terpinene 4.28 1012 9.23 3.02 1144 9.26 Carvomenthene 4.33 1016 0.01 2.48 1103 0.01 para-cymene 4.38 1019 2.61 4.16 1225 2.60 β-phellandrene 4.44* 1023 3.57 3.32 1166 1.00 Limonene 4.44* 1023 [3.57] 3.22 1159 0.80 1,8-Cineole 4.47 1025 [3.57] 3.35 1168 1.72 (Z)-β-Ocimene 4.66 1037 0.01 3.89* 1207 19.67 (E)-β-Ocimene 4.82 1047 0.02 4.03 1216 0.02 γ-terpinene 4.97 1057 19.61 3.89* 1207 [19.67] cis-sabinene hydrate 5.06 1062 0.02 6.96 1431 0.02 Terpinolene 5.40 1084 3.34 4.34 1237 3.30 trans-sabinene hydrate 5.54 1092 0.03 8.04 1511 0.03 Linalool 5.62 1098 0.06 8.13 1519 0.08 Unknown [m/z 119, 109 (94), 43 (61), 95 (56), 91 (48), 77 (32), 152 5.69 1102 0.02 8.60* 1555 1.33 (32), 137 (31), 134 (24)] para-mentha-1,3,8-5.74 1105 0.01 6.19* 1375 [0.02] Page 9/12

Borneol 6.61 1161 0.01 9.86* 1655 3.03 δ-terpineol 6.66 1164 tr 9.55 1629 0.01 Terpinen-4-ol 6.84* 1176 39.24 8.70* 1562 39.12 Dill ether 6.84* 1176 [39.24] 7.40 1463 tr para-cymen-8-ol 6.91 1180 [39.24] 11.62 1802 0.05 α-terpineol 7.00 1187 2.91 9.86* 1655 [3.03] cis-piperitol 7.05 1190 0.07 9.58 1632 0.13 Unknown [m/z 121, 43 (99), 91 (85), 77 (73), 93 (41), 136 (33)... 166 (3)] 7.13 1195 0.02 triene cis-para-menth-2- en-1-ol 5.89 1115 0.27 8.19 1523 0.28 4-Hydroxy-4- methylcyclohex-2-6.08 1128 0.02 14.11 2030 0.02 enone Cosmene isomer I 6.20* 1135 0.18 6.39 1389 0.06 trans-para-menth- 2-en-1-ol 6.20* 1135 [0.18] 9.04* 1589 0.80 Unknown [m/z 109, 124 (45), 119 (41), 43 (35), 91 (28), 95 (25)...] 6.32 1143 0.10 6.88* 1425 0.16 trans-piperitol 7.25 1202 0.10 10.42 1700 1.82 endo-fenchyl acetate 7.40 1213 0.01 6.88* 1425 [0.16] exo-2- Hydroxycineole 7.47 1218 0.02 11.71 1810 0.02 Nerol 7.67 1231 0.03 11.14 1762 0.04 Piperitone 7.88 1245 0.07 9.98 1664 0.15 cis-carvenone 8.01 1254 0.02 oxide? trans-ascaridole glycol 8.13 1262 0.05 14.24 2042 0.04 cis-ascaridole glycol? 8.40 1280 0.03 14.89 2105 0.04 Thymol 8.64 1296 0.01 15.14 2129 0.01 Carvacrol 8.74 1303 0.01 15.38 2154 0.01 Unknown [m/z 97, 112 (92), 83 (62), 43 (44), 41 (25)... 170? (4)] 8.89 1314 0.03 15.11 2127 0.03 Bicycloelemene 9.14 1332 0.03 7.09 1440 0.02 α-cubebene 9.33 1345 0.07 6.81 1420 0.07 Isoledene 9.64 1367 0.07 6.88* 1425 [0.16] α-copaene 9.67 1369 0.13 7.17 1447 0.13 7-Cubebene 9.72* 1372 0.07 7.14 1444 0.07 7-Cubebene epimer? 9.72* 1372 [0.07] 7.26 1453 0.03 β-cubebene 9.88 1384 0.03 7.77 1491 0.05 Page 10/12

β-elemene 9.92 1387 0.04 8.60* 1555 [1.33] α-gurjunene 10.13 1402 0.46 7.65 1482 0.43 β-maaliene 10.17 1405 0.01 7.81 1494 0.01 β-caryophyllene 10.24 1410 0.44 8.46 1544 0.43 γ-maaliene 10.36 1419 0.08 8.56 1551 0.10 β-gurjunene 10.41 1422 0.02 8.39 1538 0.03 α-maaliene 10.44 1425 0.08 8.70* 1562 [39.12] Aromadendrene 10.51 1430 1.40 8.60* 1555 [1.33] Selina-5,11-diene 10.57 1435 0.18 8.74 1566 0.23 trans-muurola-3,5- diene 10.67 1442 0.15 8.91 1579 0.14 α-humulene 10.70 1444 0.10 9.32 1611 0.10 allo- Aromadendrene 10.80* 1452 0.64 9.04* 1589 [0.80] Valerena-4,7(11)- diene 10.80* 1452 [0.64] 9.01 1586 0.02 γ-gurjunene 10.97 1464 0.06 9.18 1600 0.08 trans-cadina- 1(6),4-diene 11.00* 1467 0.39 9.28 1608 0.35 Selina-4,11-diene 11.00* 1467 [0.39] 9.46 1622 0.03 γ-muurolene 11.04 1470 0.04 9.71 1643 0.05 β-selinene 11.13 1477 0.12 9.90 1658 0.13 allo-aromadendr- 9-ene 11.17 1479 0.12 9.62 1635 0.10 trans-muurola- 4(15),5-diene 11.21 1482 0.10 9.86* 1655 [3.03] δ-selinene 11.24 1484 0.13 9.69* 1641 1.20 Viridiflorene 11.28* 1488 2.13 9.69* 1641 [1.20] Bicyclogermacrene 11.28* 1488 [2.13] 10.10 1674 0.95 α-selinene 11.28* 1488 [2.13] 10.02 1667 0.03 α-muurolene 11.36 1494 0.19 10.07 1672 0.16 γ-cadinene 11.52 1506 0.04 10.46* 1704 [1.82] trans-calamenene 11.64 1516 0.11 11.27 1772 0.13 Zonarene 11.67* 1518 1.74 10.46* 1704 [1.82] δ-cadinene 11.67* 1518 [1.74] 10.46* 1704 [1.82] trans-cadina-1,4- diene 11.76 1525 0.23 10.70 1724 0.25 α-calacorene 11.87 1534 0.02 12.17 1850 0.03 Eudesma-5,7(11)- diene 12.14 1555 0.02 11.16 1763 0.03 Unknown [m/z 161, 109 (98), 82 (93), 43 (72), 105 (68), 93 (59), 69 12.16 1557 0.13 13.34 1956 0.12 (56), 119 (55)... 222 (7)] Spathulenol 12.30 1568 0.10 14.46 2062 0.11 Globulol 12.38 1574 0.40 13.96 2015 0.38 Gleenol 12.44 1578 0.04 13.63 1983 0.04 Viridiflorol 12.47 1581 0.19 14.04 2023 0.19 Cubeban-11-ol 12.51 1584 0.16 13.74* 1994 0.26 Ledol 12.61* 1592 0.15 13.42 1964 0.06 Page 11/12

Eudesm-5-en-11-ol analog 12.61* 1592 [0.15] 14.28 2045 0.09 10-epi-Cubenol 12.75 1603 0.01 Rosifoliol 12.87 1613 0.15 14.38 2055 0.16 1-epi-Cubenol 12.95 1619 0.22 13.82 2002 0.24 Isospathulenol 13.06 1629 0.05 15.50 2166 0.05 Cubenol 13.12 1634 0.13 13.74* 1994 [0.26] α-muurolol 13.17 1638 0.05 15.25 2141 0.06 Total identified 98.72% 98.73% Total reported 99.00% 98.87% *: Two or more compounds are coeluting on this column [xx]: Duplicate percentage due to coelutions, not taken account in the identified total : Peaks apexes were resolved, but peaks overlapped and were summed for analysis tr: The compound has been detected below 0.005% of total signal. Note: no correction factor was applied R.T.: Retention time (minutes) R.I.: Retention index Page 12/12