Supplementary Material. Portable near infrared spectroscopy (micronir) applied to abuse drugs. and medicines analyzes
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1 Electronic Supplementary Material (ESI) for Analytical Methods. This journal is The Royal Society of Chemistry 2018 Supplementary Material Portable near infrared spectroscopy (micronir) applied to abuse drugs and medicines analyzes Radigya M. Correia, a Eloilson Domingos, a Flavia Tosato, a Nayara A. dos Santos, a Julia de A. Leite, a Mayara da Silva, a Marcelo C. A. Marcelo, b Rafael S. Ortiz, c,d Paulo R. Filgueiras, a Wanderson Romão a,d,e * a Laboratório de Petroleômica e Química Forense, Departamento de Química, Universidade Federal do Espírito Santo, Vitória ES, Brazil. b Instituto de Química, Universidade Federal do Rio Grande do Sul, Porto Alegre, Rio Grande do Sul, Brazil. c Setor Técnico-Científico, Superintendência Regional do Departamento de Polícia Federal no Rio Grande do Sul, Brazil. d Instituto Nacional de Ciência e Tecnologia Forense (INCT Forense), Brazil. e Instituto Federal do Espírito Santo, Vila Velha ES, Brazil.
2 Table 1S. Active ingredients identified by CG-MS analysis Samples Active ingredient identified by CG-MS C 1 Amphetamine, FA, Methamphetamine,, and 2CB C 2 Amphetamine, and caffeine C 3 Amphetamine, and caffeine C 4 C 5 C 6 C 7 C 8 C 9 C 10 C 11 C 12 C 13 C 14 C 15 C 16 C 17 C 18, and Ethylone C 19 MDA
3 Table 2S.. m/z values, mass error (ppm), DBE, empirical formula and proposed structures for the signals detected from PS(+)MS analysis for designer drugs samples. Samples Proposed structures [M+H] + measured m/z theoretical m/z Error (ppm) DBE 25I-NBOMe [C 18 H 22 INO 3 +H] S 1 25B-NBOMe [C 18 H 22 BrNO 3 +H] C-NBOMe [C18H22ClNO3+H] S 2 25I-NBOMe [C 18 H 22 INO 3 +H] S 3 25I-NBOMe [C 18 H 22 INO 3 +H] S 4 25I-NBOMe [C 18 H 22 INO 3 +H] S 5 25I-NBOMe [C 18 H 22 INO 3 +H] S 6 25I-NBOMe [C 18 H 22 INO 3 +H] S 7 25I-NBOMe [C 18 H 22 INO 3 +H] S 8 25I-NBOMe [C 18 H 22 INO 3 +H] S 9 25I-NBOMe [C 18 H 22 INO 3 +H] S 10 25I-NBOMe [C 18 H 22 INO 3 +H] S 11 25I-NBOMe [C 18 H 22 INO 3 +H] S 12 25I-NBOMe [C 18 H 22 INO 3 +H] S 13 S 14 S 15 S 16 25I-NBOMe [C 18 H 22 INO 3 +H] S 17 LSD* S 18 LSD* S 19 25I-Nbome* S 20 25I-Nbome* DOC [C 11 H 16 ClNO 2 +H] S 21 25I-NBOMe [C 18 H 22 INO 3 +H] DOC [C 11 H 16 ClNO 2 +H] S 22 25I-NBOMe [C 18 H 22 INO 3 +H] *Active ingredients were identified by thin layer chromatography in samples S 17 -S 20.
4 Table 3S. Chemical composition of Desobesi-M, Sibutramina, Pramil, Erofast, Dualid- S e Fingrass medicines obtained from GC-MS analysis. Compostion Sample Label Active principle Compound found Report Dualid-S Dualid-S Amfepramone hydrochloride Fluoxetine Dualid-S Dualid-S Amfepramone hydrochloride Fluoxetine Sibutramina Sibutramina Sibutramina Sibutramina Sibutramina Sibutramina Fingrass Fingrass Fingrass Fingrass Erofast Erofast Sildenafil Sildenafil Sibutramina Sibutramina Benzocaine/caffeine nacional
5
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