Address: Attn: Tel: Client: e-mail: Code: The following sample was (were) submitted and identified by the client as: Sample description: RAW MATERIAL Batch No.: Job no Report No.: 17-010610 Reference No.: SALMON FLAME Composition indicated: UNKNOWN Serie : Receiving Date: 06/07/2017 Test Start Date: 08/07/2017 Test End Date: 19/07/2017 SOP description s * SOP 2 - Colour fastness to artificial light for fabrics - Xenom lamp * SOP 2-Determination of arylamines for natural samples SOP 8-Determination of formaldehyde by photometric in textile samples (DC) * SOP 70-Determination of allergenous dyes SOP -Determination of cadmium and lead in textile samples by ICP-MS * SOP 20-Determination of the content of phenols SOP 60-Colour Fastness to Rubbing (Direct Contact) SOP 62-Colour Fastness to Acid perspiration (Direct contact) SOP 62-Colour Fastness to Alkaline perspiration (Direct contact) SOP 13 - Colour fastness to domestic washing C06 *SUMMARY OF TEST CONCLUSIONS Sample Tested Pag. 1 of 9
* 20 SOP 2 - Colour fastness to artificial light for fabrics - Xenom lamp AMSLab S-170708-00133 S-170708-00133 Colour change Blue Scale 7/8 Hours test process 30 - Applied standard based in UNE-EN ISO 10-B02:2001 (Equivalent to ISO 10-B02:1994) - NA = not applicable Note 1: Used Blue scale from 1 to 8. * 20 SOP 2-Determination of arylamines for natural samples Composite Sample S-170711-00743 (N = 6) AMSLab 6 S-170711-00664 S-170711-00743 0-dianisidine (3,3-dimethoxybenzidine) 119-90-4 n.d. 2,4,-trimethylaniline 137-17-7 n.d. 2,4-Diaminotoluene 9-80-7 n.d. 2,4-dimethylaniline 9-68-1 n.d. 2,6-dimethylaniline 87-62-7 n.d. 2-Nafthylamine 91-9-8 n.d. 3,3-dichlorobenzidine 91-94-1 n.d. 3,3-dimethylbenzidine 119-93-7 n.d. 4,4-Diaminediphenyl sulfide 139-6-1 n.d. 4,4-Oxydianiline 101-80-4 n.d. 4,4-diaminophenylmethane 101-77-9 n.d. 4,4-methylen-bis-(2-Chloroaniline) 101-14-4 n.d. 4,4-methylendi-o-toluidine 838-88-0 n.d. 4-Aminoazobenzene 60-09-3 n.d. Pag. 2 of 9
S-170711-00743 4-Aminobiphenyl 92-67-1 n.d. 4-Chloro-o-toluidine 9-69-2 n.d. 4-Chloroaniline 106-47-8 n.d. 4-Methoxy-m-phenilenediamine 61-0-4 n.d. -Nitro-o-toluidine 99--8 n.d. 6-methoxy-m-toluidine 120-71-8 n.d. Benzidine 92-87- n.d. o-aminoazotoluene 97-6-3 n.d. o-anisidine 90-04-0 n.d. o-toluidine 9-3-4 n.d. - Applied standard UNE-EN 14362-1:2012 - Requirement by the client= 20 mg Kg-1 for textile 30 mg Kg-1 for leather goods - (Nº=..) = number of subsamples included. If N>number of subsamples visible, in this composite sample it mixed different references by customer indications. Test Report Unit: mg Kg-1 n.d.= not detected (<MDL) MDL (Method Detection Limit )= 1,0 mg Kg-1 82 SOP 8-Determination of formaldehyde by photometric in textile samples (DC) Composite Sample S-170711-0074 (N = 6) AMSLab 7 S-170711-0066 Formaldehyde 0-00-00 S-170711-0074 Pag. 3 of 9
- Applied standard ITX-GB/T 2912.1/2012 7 mg Kg-1 for items of direct contact 300 mg Kg-1 garment with indirect contact - (Nº=..) = number of subsamples included. If N>number of subsamples visible, in this composite sample it mixed different references by customer indications. Test Report Unit: mg Kg-1 n.d.= not detected = <LOQ LOQ (Limit of quantification )= 2,0 mg Kg-1 * 700 SOP 70-Determination of allergenous dyes 8 AMSLab S-170711-00666 S-170711-00666 Disperse Blue 1 247-4-8 n.d. Disperse Blue 102 12222-97-8 n.d. Disperse Blue 106 12223-01-7 n.d. Disperse Blue 124 6191-1-7 n.d. Disperse Blue 26 3860-63-7 n.d. Disperse Blue 3 247-46-9 n.d. Disperse Blue 3 624-77-7 n.d. Disperse Blue 7 3179-90-6 n.d. Disperse Brown 1 233-64-8 n.d. Disperse Orange 1 281-69-3 n.d. Disperse Orange 3 730-40- n.d. Disperse Orange 37 13301-61-6 n.d. Disperse Red 1 2872-2-8 n.d. Disperse Red 11 2872-48-2 n.d. Disperse Red 17 3179-89-3 n.d. Disperse Yellow 1 119-1-3 n.d. Disperse Yellow 3 2832-40-8 n.d. Disperse Yellow 39 12236-29-2 n.d. Disperse Yellow 49 4824-37-2 n.d. Disperse Yellow 9 6373-73- n.d. - Applied standard DIN 4231 - Requirement by the client= 0,0 mg Kg-1 Pag. 4 of 9
Test Report Unit: mg Kg-1 n.d.= not detected (<MDL) MDL (Method Detection Limit )= 1,0 mg Kg-1 0 SOP -Determination of cadmium and lead in textile samples by ICP-MS Composite Sample S-170711-0071 (N = 4) AMSLab 10 S-170711-00668 S-170711-0071 Cadmium 7440-43-9 n.d. Lead 7439-92-1 n.d. - Applied standard CPSC-CH-E1002-08.3 (2012) 7,0 mg Kg-1 for cadmium 100,0 mg Kg-1 for lead Test Report Unit: mg Kg-1 n.d.= not detected = <LOQ LOQ (Limit of quantification )= 0,0 mg Kg-1 Pag. of 9
* 200 SOP 20-Determination of the content of phenols 9 AMSLab S-170711-00667 S-170711-00667 PCP 87-86- n.d. TeCP 2167-83-3 n.d. - Requirement by the client= 0,0 mg Kg-1. Test Report Unit mg Kg-1 n.d= not detected (<MDL) MDL (Method Detection Limit )= 0,0 mg Kg-1 600 SOP 60-Colour Fastness to Rubbing (Direct Contact) 1 AMSLab S-170708-00129 Cross Staining S-170708-00129 Length direction Dry Colour Change Length direction Dry Staining 4/ Length direction Wet Colour Change 4/ Length direction Wet Staining 2/3 (**) Width direction Dry Colour Change Width direction Dry Staining 4/ Width direction Wet Colour Change 4/ Width direction Wet Staining 2/3 (**) - Applied standard UNE-EN ISO 10-X12:2016 (Equivalent to ISO 10-X12:2016) 3 in Grey Scale ISO 10-A02 for Colour Change 3 in Grey Scale ISO 10-A03 for Colour Staining. - Requirement by the client, products intended for children under 3 years= 4 in Grey Scale ISO 10-A02 for Colour Change 4 in Grey Scale ISO 10-A03 for Colour Staining. - = not applicable Pag. 6 of 9
Test Note 1: Rubbing plug with a cylinder of (16 ± 0.1) mm, which apply a downward force of (9 ± 0.2) N Note 2: Only for Hair fabrics: Rubbing plug with a rectangular area of 19 mm x 2.4 mm, which apply a downward force of (9 ± 0.2) N Note 3: Adjacent Fabric Monofibre used: Cotton Note 4: Impregnation/absorption percentage for wet rubbing: 9-100 % Note : Conditioning time for analyzed fabrics and adjacent fabrics: 4 hours Note 6: Environmental conditions: (20±2) ºC and (6±2) % of RH 621 SOP 62-Colour Fastness to Acid perspiration (Direct contact) 2 AMSLab S-170708-00130 S-170708-00130 Colour Change Cross Staining Staining Acetate Staining Acrylic Staining Cotton Staining Linen Staining Polyamide Staining Polyester Staining Silk Staining Viscose Staining Wool - Applied standard UNE-EN ISO 10-E04:2013 (Equivalent to ISO 10-E04:2013) 3 in Grey Scale ISO 10-A02 for Colour Change 3 in Grey Scale ISO 10-A03 for Colour Staining. - Requirement by the client, products intended for children under 3 years= 3-4 in Grey Scale ISO 10-A02 for Colour Change 3-4 in Grey Scale ISO 10-A03 for Colour Staining. - = not applicable Test Note 1: Acid solution used with ph. (± 0.2) Note 2: Adjacent Fabric Monofibre used: if only appear two results in staining Note 3: Adjacent Fabric Multifibre type used: DW, see results if appear more than two results in staining. Note 4: Perspirometer position for test: Vertical Pag. 7 of 9
622 SOP 62-Colour Fastness to Alkaline perspiration (Direct contact) 3 AMSLab S-170708-00131 S-170708-00131 Colour Change Cross Staining Staining Acetate Staining Acrylic Staining Cotton Staining Linen Staining Polyamide Staining Polyester Staining Silk Staining Viscose Staining Wool - Applied standard UNE-EN ISO 10-E04:2013 (Equivalent to ISO 10-E04:2013) 3 in Grey Scale ISO 10-A02 for Colour Change 3 in Grey Scale ISO 10-A03 for Colour Staining. - Requirement by the client, products intended for children under 3 years= 3-4 in Grey Scale ISO 10-A02 for Colour Change 3-4 in Grey Scale ISO 10-A03 for Colour Staining. - = not applicable Test Note 1: Alkaline solution used with ph 8 (± 0.2) Note 2: Adjacent Fabric Monofibre used: if only appear two results in staining Note 3: Adjacent Fabric Multifibre type used: DW, see results if appear more than two results in staining. Note 4: Perspirometer position for test: Vertical 130 SOP 13 - Colour fastness to domestic washing C06 4 AMSLab S-170708-00132 S-170708-00132 Colour Change Cross Staining Staining Acetate Pag. 8 of 9
TEST REPORT Date: 19/07/2017 Staining Acrylic Staining Cotton Staining Linen Staining Polyamide Staining Polyester Staining Silk Staining Viscose Staining Wool Washing Temperature S-170708-00132 30ºC - Applied standard UNE-EN ISO 10-C06:2010 (Equivalent to ISO 10-C06:2010) - = not applicable - Requirement recommended= 3 in Grey Scale ISO 10-A02 for Colour Change 3 in Grey Scale ISO 10-A03 for Colour Staining. Test Note 1: Test Temperature: Indicated in results table Note 2: Test number according with Tª: A1S (40ºC - 30 min) / A1M (40ºC - 4 min) / B1S (0ºC - 30 min) / B1M (0ºC - 4 min) / C1S (60 ºC 30 min) / C1M (60 ºC - 40 min) Note 3: Steel balls used: Yes Note 4: Treatment with acetic acid: No Note : Detergent used: ECE phosphate reference detergent (B) Note 6: Adjacent Fabric Monofibre used: if only appear two results in staining Note 7: Adjacent Fabric Multifibre type used: DW, see results if appear more than two results in staining. Issue Signed: Manuel Lolo Signed: Pablo Perez General Manager Chemical Lab Manager Signed: Esteban Ramirez Physical Lab Manager Pag. 9 of 9